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Product Details
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Uses |
4-Iodo-1-tritylimidazole is a compound useful in organic synthesis. |
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Chemical Properties |
White Solid |
InChI:InChI=1/C22H17IN2/c23-21-16-25(17-24-21)22(18-10-4-1-5-11-18,19-12-6-2-7-13-19)20-14-8-3-9-15-20/h1-17H
The invention belongs to the technical f...
The present application belongs to the f...
Indoleamine 2,3-dioxygenase (IDO) 1 is t...
The present invention relates to O-GIcNA...
4-iodoimidazole
trityl chloride
N-trityl-4(5)-iodoimidazole
| Conditions | Yield |
|---|---|
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With triethylamine; In N,N-dimethyl-formamide; at 20 - 25 ℃; for 22h; Solvent; Reagent/catalyst; Temperature;
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97.2% |
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With triethylamine; In N,N-dimethyl-formamide; Ambient temperature;
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95% |
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With triethylamine; In N,N-dimethyl-formamide; at 20 ℃; for 24h;
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94% |
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With triethylamine; In N,N-dimethyl-formamide; at 20 ℃; for 24h;
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94% |
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With triethylamine; In DMF (N,N-dimethyl-formamide); at 20 ℃; for 48h;
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93% |
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With triethylamine; In DMF (N,N-dimethyl-formamide); at 20 ℃; for 48h;
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93% |
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With triethylamine; In dichloromethane; at 25 ℃; for 17h; Cooling with ice; Inert atmosphere;
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93% |
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With triethylamine; In dichloromethane; at 25 ℃; for 17h; Inert atmosphere;
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93% |
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With triethylamine; In dichloromethane; at 25 ℃; for 17h; Inert atmosphere;
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93% |
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In DMF (N,N-dimethyl-formamide); at 20 ℃; for 24h;
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92% |
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4-iodoimidazole; With triethylamine; In N,N-dimethyl-formamide; at 0 ℃; for 0.166667h;
trityl chloride; In N,N-dimethyl-formamide; at 20 ℃; for 16h;
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92% |
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In ISOPROPYLAMIDE; at 0 - 20 ℃;
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90% |
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With triethylamine; In N,N-dimethyl-formamide; at 20 ℃; for 48h;
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88.9% |
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With triethylamine; In dichloromethane; at 20 ℃; for 15h;
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88% |
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With triethylamine; In tetrahydrofuran; at 70 ℃; for 3h; Inert atmosphere;
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81% |
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With N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 20 ℃;
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78% |
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With triethylamine; In N,N-dimethyl-formamide; Ambient temperature;
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76% |
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With triethylamine; In tetrahydrofuran; at 80 ℃;
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71% |
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With triethylamine; In N,N-dimethyl-formamide; at 20 ℃; for 14h;
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66% |
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With triethylamine; In tetrahydrofuran; for 1.5h; Reflux;
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64% |
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With triethylamine; In water; N,N-dimethyl-formamide;
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59% |
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4-iodoimidazole; With triethylamine; In dichloromethane; at 20 ℃; for 0.0833333h;
trityl chloride; In dichloromethane; at 40 ℃; for 16h;
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58% |
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With triethylamine; In tetrahydrofuran; at 70 ℃; for 3h;
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55.57% |
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With triethylamine; In tetrahydrofuran;
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With triethylamine; In dichloromethane;
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With triethylamine; In N,N-dimethyl-formamide;
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With triethylamine; In N,N-dimethyl-formamide; at 20 ℃; for 16h;
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4-iodoimidazole
diethyl ether
trityl chloride
N-trityl-4(5)-iodoimidazole
| Conditions | Yield |
|---|---|
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In N,N-dimethyl-formamide;
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92% |
4-iodoimidazole
trityl chloride
diethyl ether
5-Hydroxy-5-(1-trityl-1H-imidazol-4-yl)-pentanoic acid methyl ester
1,1-Bis(methylthio)-2-fluoro-3-((1'-trityl)-4'-imidazolyl)prop-1-en-3-ol
1-triphenylmethyl-4-[(1-hydroxy-1-phenyl)methyl]-1H-imidazole
alpha-methyl-1-triphenylmethyl-1H-imidazole-4-methanol
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